heated to about 85oC it was kept at this temperature for about 10 minutes, it did not go over this temperature as if it did the compound may of decomposed. The crystals are so dissolved in 5ml of ethyl alcohol. Problems, which may occur The problems, which may occur, are: * When refluxing the mixture the water bath may not be hot enough and the reaction may not take place. The visual aspect of ASA is an odourless, white, acerate and glistening solid. The mixture was cooled in an ice/water bath, and then the mixture was poured in to 150 cm3 of cold deionised water in a 250 cm3 beaker. Measure mass of aspirin.
Preparation, of, aspirin, essay, example for Free Preparation, and Recrystallisation Of, aspirin, biology, essay
Apply suction using a filter pump and wash the crystals with ice cold water. Recrystallise the product from hot water and determine its melting point. The crystals were dried in an oven at about 100 oC and then the clock glass and crystals reweighed. Theory, esters are organic compounds with the general expression rcoor, where Roentgen and R steps to writing an exploratory essay can be an alkyl group or an aromatic group. However, Acetic anhydride is preferred because it is less risky to utilize and less expensive than acetyl chloride.
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